Acid Deposition: Proceedings of the CEC Workshop organized by Prof. J. Schmoelling (auth.), S. Beilke, A. J. Elshout

By Prof. J. Schmoelling (auth.), S. Beilke, A. J. Elshout (eds.)

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Extra resources for Acid Deposition: Proceedings of the CEC Workshop organized as part of the Concerted Action “Physico-Chemical Behaviour of Atmospheric Pollutants”, held in Berlin, 9 September 1982

Sample text

2. Establishing the presence of weak acids in a natural water The method presented here is based on Gran's plot. (1) Suppose a naturruwater sample is titrated with NaOH in such a way as to keep the volume of the sample (almost) constant. The NaOH-solution is ~dded in equal doses and [H+l is measured after every addition. [H+] is finally plotted against [OWJadd in a diagram. As has been shown by the author (2) the slope (m) of the curve obtained in this way is given by the following expression: d rH+' .

The second is the titration procedure discussed in the last section. Details concerning this method are presented elsewhere (4). However, it is important to remember that all data must be obtained in terms of concentrations. They should correspond to points within the relevant - [H+] -range (10- 3 - 10- 5 mole 1- 1). 10 mole 1- 1 KCl and a [H+J>10-4 mol e 1- 1• Next CO is removed by bubbling N2 through the solution to facilitate the dete~ination of other weak acids if present. 0100 mole 1- 1 NaOH by means ofa microburette.

Lee and the author (~) and~ incfuding some new points of view, by the author (7). However, a short presentation and discussion of this diagram are in order here. Fig. 1 shows the diagram. 1\ ,,~ ... ". ~4pPbNH3 " I \ I ,'1\\\ )' \ \ \ '\ ',99 .... h. O) has been proposed by Tang et al. (8). ). H. Lee (6). The solubility curve is based on data given by d'Ans (9). The solid phases have been identified in aerosol particles by the author (10). i~~ __ ~l:~g:~~ The points 51, 52, 53 represent the solid phases (NH4)2504' (NH 4)3 H(50 4)2 and NH 4H50 4.

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